Detalle Publicación

ARTÍCULO

Evolution of the Magnetic Properties of Co10Cu90 Nanoparticles Prepared by Wet Chemistry with Thermal Annealing

Autores: Garcia, I.; Etxeberria Uranga, Jon Joseba; Kakazei, G.N.; Golub, V.O.; Saliuk, O.Y.; Ilyn, M.; Guslienko, K.Y.; Gonzalez, J.M.
Título de la revista: JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY
ISSN: 1533-4880
Volumen: 12
Número: 9
Páginas: 7529 - 7534
Fecha de publicación: 2012
Resumen:
Nanoparticles of Co10Cu90 alloy have been prepared by sonochemical wet method. According to transmission electron microscopy, bimetallic particles with typical diameter of 50-100 nm consisting of nanocrystallites with average diameter of 15-20 nm were obtained. The samples were annealed at 300 degrees C and 450 degrees C. Zero field cooled and field cooled temperature dependences of magnetization in the temperature range of 5-400 K at 50 Oe, as well as magnetization hysteresis loops at 15, 100 and 305 K were measured by vibrating sample magnetometry. Presence of antiferromagnetic phase, most probably of the oxide Co3O4, was observed in as-prepared sample. The lowest coercivity was found for the CoCu sample annealed at 300 degrees C, whereas for as prepared sample and the one annealed at 450 degrees C it was significantly higher. The samples were additionally probed by continuous wave ferromagnetic resonance at room temperature using a standard X-band electron spin resonance spectrometer. A good correspondence between evolution of the coercivity and the microwave resonance fields with annealing temperature was observed.
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