Revistas
Revista:
REVISTA ESPAÑOLA DE MECÁNICA DE LA FRACTURA
ISSN:
2792-4246
Año:
2022
N°:
3
Págs.:
95 - 100
Wire drawing parameters such as area reduction and die angle have an important effect on damage generation. One of the most common defects appearing under certain critical configurations are the so-called ¿chevron cracks¿. These defects are difficult to identify since they are typically located at the wire core. To address this, great efforts have been made in the last two decades to develop numerical models capable of predicting damage evolution and failure. Continuum Damage Mechanics (CDM) models present the advantage of being coupled with the constitutive behaviour of the material. Among these models, Lemaitre¿s approach is one of the most widely used. In its original formulation, the model did not
distinguish between tension and compression stresses in terms of damage accumulation. An additional parameter was then included to consider the crack closure effect under compressive stresses. However, this formulation is not valid for wire drawing, since it overestimates damage under these conditions. For this reason, a new damage model following Lemaitre¿s approach has been derived by redefining the crack closure effect under compressive stresses. In this way, under high hydrostatic compressive stresses, such as in the case of wire drawing, the model yields more realistic results in terms of damage accumulation. The model has been implemented in ABAQUS through user subroutines UMAT (for implicit cases) and VUMAT (for explicit cases). Single-pass wire drawing simulations have been performed to compare the original model with the new formulation.
Autores:
Dorronsoro, A. (Autor de correspondencia); Páez, J. R.; Navarrete, J.; et al.
Revista:
REVISTA ESPAÑOLA DE MECÁNICA DE LA FRACTURA
ISSN:
2792-4246
Año:
2022
N°:
4
Págs.:
89 - 94
In many practical situations, the distribution of residual stresses can have a paramount influence on the fatigue and fracture response of materials. In this paper, we describe a method for the local measurement of residual stresses. It consists of Digital Image Correlation (DIC) of Scanning Electron Microscope (SEM) images of a surface, before and after milling a slit using a Focused Ion Beam (FIB). The DIC algorithm used in this work is based on Fourier analysis, which can reach sub-pixel resolution. In order to calculate the internal stresses released during the milling process, the displacements detected with the DIC algorithm are fitted to Finite Element Method (FEM) simulations. Residual stresses measured by this method on a hard metal sample subjected to different laser surface treatments are successfully compared with X-ray diffraction measurements.
Autores:
Pérez, B. (Autor de correspondencia); Bergara, A.; Bre, A.; et al.
Revista:
NUCLEAR MATERIALS AND ENERGY
ISSN:
2352-1791
Año:
2022
Vol.:
30
Págs.:
101124
Flow Channel Inserts (FCIs) are key elements in the high temperature DCLL blanket concept since they provide the required thermal insulation between the He-cooled structural steel and the hot PbLi flowing at a maximum temperature of 700 ?, and the necessary electrical insulation to minimize magnetohydrodynamic (MHD) effects. In this paper, the use of SiC-sandwich material for FCIs consisting of a porous SiC core (thermal and electrical insulator) covered by a dense Chemical Vapor Deposition (CVD) SiC layer (protection against PbLi infiltration) has been studied. Lab-scale FCI prototypes were produced by the gel casting method and characterized in terms of thermal and electrical conductivities (the latter before and after exposure to ionizing radiation) and flexural strength. Corrosion tests under flowing PbLi at 500-700 ?& nbsp;in presence of a magnetic field up to 5 T were performed obtaining promising results regarding the reduction of MHD pressure drop and the compatibility of SiC and PbLi under dynamic conditions. Additionally, thermomechanical finite elements simulations were performed in a 3D channel geometry to identify black spots regarding thermal stresses.
Autores:
Bergara, A. (Autor de correspondencia); Arredondo, A.; Altuzarra, J.; et al.
Revista:
OCEAN ENGINEERING
ISSN:
0029-8018
Año:
2022
Vol.:
257
Págs.:
111605
The main objective of this work has been the validation of a methodology to assess fatigue crack propagation in offshore mooring chains under service conditions. For this purpose, analytical Stress Intensity Factor (SIF) solutions with step-by-step application of the Paris law and the Extended Finite Element Method (XFEM) implemented in the Abaqus (R) 2018 software have been studied. The fatigue crack propagation analysis is divided in two stages. First, a static analysis-pre-stretch and subsequent unloading-representative of the manufacturing process is performed. Next, the fatigue crack propagation simulation is performed under simplified loading conditions and taking into account the residual stresses induced in the previous analysis. Finally, analytical solutions, numerical simulations and experimental results have been compared. Results justify the use of the Extended Finite Element Method (XFEM) for fatigue crack propagation analysis in mooring chains.
Autores:
Bergara, A. (Autor de correspondencia); Dorado, J. I. ; Martín, Antonio; et al.
Revista:
MECHANICS OF ADVANCED MATERIALS AND STRUCTURES
ISSN:
1537-6494
Año:
2021
Vol.:
28
N°:
8
Págs.:
861-873
This work presents the numerical modeling and validation of two different fatigue propagation tests that attempt to simulate the crack growth situation that takes place at aeronautic engine vane guides. These vanes, which are cylindrical skins of very thin thickness (few millimeters), are responsible for holding the static blades of both the compressor and the turbine. The union of discs and blades is a very conflictive zone due to high stresses and possible manufacturing defects. The first test designed for this work tries to reproduce crack growth at geometric discontinuities and sharp edges, such as the union between the disc and the blades. The second test tries to reproduce the crack growth situation that takes place in skins of very thin thickness, such as vane guides. First, the experimental set-ups as well as the experimental results are presented. Then, the numerical FE models and simulations -corresponding to the experimental tests that have been performed- are explained. Finally, the comparison between the experimental and numerical results is presented. Crack growth was controlled by optical microscopy and by progressive crack surface heat-tinting. For the numerical simulations, the Extended Finite Element Method (XFEM) implemented in Abaqus (R) 2017 software has been used. The comparison between the experimental and numerical results shows very good correlation regarding crack shape and number of cycles until failure. The capabilities of the XFEM-based LEFM approach to simulate fatigue crack growth in complex crack fronts are validated.
Revista:
INTERNATIONAL JOURNAL OF FATIGUE
ISSN:
0142-1123
In this article, multiaxial fatigue space, fatigue basic unit and fatigue damage map are proposed, as well as out-of phase failure angle and out-of-phase level coefficient. The comprehensive discussion of out-of-phase failure is conducted, it is found that the relative distortion deformation is a proper reflection for out-of-phase failure and it has a limit effect. The validation with 394 samples of 13 materials under 37 loading conditions indicates that the proposed theory has an excellent universal capability with minimum prediction error and favorable error distribution, the prediction ability is improved by 21.1% compared with original Lu criterion.
Revista:
APPLIED SCIENCES
ISSN:
2076-3417
Año:
2021
Vol.:
11
N°:
3
Págs.:
1026
Rolling contact fatigue (RCF) is a common cause of rail failure due to repeated stresses at the wheel-rail contact. This phenomenon is a real problem that greatly affects the safety of train operation. Preventive and corrective maintenance tasks have a big impact on the Life Cycle Cost (LCC) of railway assets, and therefore cutting-edge strategies based on predictive functionalities are needed to reduce it. A methodology based on physical models is proposed to predict the degradation of railway tracks due to RCF. This work merges a crack initiation and a crack growth model along with a fully nonlinear multibody model. From a multibody assessment of the vehicle-track interaction, an energy dissipation method is used to identify points where cracks are expected to appear. At these points, crack propagation is calculated considering the contact conditions as a function of crack depth. The proposed methodology has been validated with field measurements, conducted using Eddy Currents provided by the infrastructure manager Network Rail. Validation results show that RCF behavior can be predicted for track sections with different characteristics without the necessity of previous on-track measurements.
Revista:
POWDER TECHNOLOGY
ISSN:
0032-5910
Año:
2021
Vol.:
381
Págs.:
92 - 100
The results of existing constitutive models describing the behaviour of metal powder during compaction processes are very different. This reveals the high sensitivity of the mechanical behaviour of porous materials to the shape, arrangement and distribution of particles and pores. In order to clarify these discrepancies, the compaction behaviour under hydrostatic loads and high temperatures for a Nickel-based superalloy has been characterized. For this characterization, a numerical optimization procedure has been defined. In parallel, finite element models at a mesoscopic level have been built with the aim of estimating the parameters that define the mechanical behaviour of metallic powder under hydrostatic loads. Then a homogenization procedure has been used to compute the macroscopic behaviour of the powder. The results of both the experimental characterization and the mesoscopic models emphasize the limits of the analysed literature constitutive models to reproduce the compaction behaviour of the considered Astroloy powder.
Revista:
VEHICLE SYSTEM DYNAMICS
ISSN:
0042-3114
Año:
2020
Vol.:
58
N°:
2
Págs.:
229 - 248
A full explicit FEM simulation of wheelset passing through switch panel is presented. The real 3D geometry of the switch panel is used, both vertical and lateral response are taken into consideration. The dynamic interaction is analysed and it is found that the damage mechanism on the switch blade and stock rail is a complex interaction of wear, fatigue and impact, which can be well described by explicit FEM simulation. Parametric analysis of running speed, traction coefficient and the friction coefficient between switch blade gauge surface and wheel flange indicate that decreasing running speed can help to reduce the damage on switch panel. The traction coefficient has little influence on the maximum impact response, but a higher traction coefficient is beneficial for eliminating the dynamic response after the maximum impact response point. The influence of the friction coefficient on the dynamic impact response is not significant, but a lower friction coefficient is favourable for decreasing the wear damage on the switch blade and increasing running safety. This work can provide a good understanding of the interaction on switch panel and give theoretical support for maintenance and improving the design.
Autores:
Bergara, A. (Autor de correspondencia); Arredondo, A.; Altuzarra, J. ; et al.
Revista:
OCEAN ENGINEERING
ISSN:
0029-8018
The main objective of this work has been the validation of a methodology to calculate the Stress Intensity Factors (SIFs) in prospective cracks of offshore mooring chains under service conditions. For this purpose, the analytic methods described in the B57910 have been compared with those calculated by the conventional Finite Element Method (FEM) by means of contour integrals and by the Extended Finite Element Method (XFEM) implemented in the Abaqus 2018 software. First, an axially loaded cylinder has been studied in order to determine the correlation between different methods for a simple case, as well as to establish the most suited finite element methodology. Then, the real case of a mooring chain has been studied, including the residual stresses induced in the manufacturing process. Finally, numerical simulations and experimental results have been compared. Results justify the use of numerical methods, specifically the use of contour integrals, for the calculation of Stress Intensity Factors (SIFs) in offshore mooring chains.
Revista:
FATIGUE AND FRACTURE OF ENGINEERING MATERIALS AND STRUCTURES
ISSN:
8756-758X
Año:
2020
Vol.:
43
N°:
1
Págs.:
137 - 148
Stochastic fatigue damage of a metro switch blade is studied with a combination of explicit finite element model (FEM), multiaxial fatigue criterion, and statistical analysis. The explicit FEM is used to reproduce dynamic procedure and to provide detailed stress/strain state variation. A multiaxial fatigue criterion proposed recently is extended to 3D conditions for fatigue prediction. The influence of stochastic impact position is considered by statistical analysis. After analysis, the formation of the serious unstable crack (continuous bites) on the switch blade can be revealed. From the perspective of service life, increasing traction coefficient and decreasing friction coefficient between wheel flange and switch blade gauge surface are beneficial but not significant. However, a speed increase from 36 to 54 km/h can lead to 40% reduction in service life. This work enhances the cognition of damage mechanism on switch blade and provides theoretical foundation for service life design and maintenance operation.
Revista:
MATERIALS SCIENCE
ISSN:
1068-820X
Año:
2019
Vol.:
55
N°:
3
Págs.:
337 - 344
A new fatigue parameter is proposed, which provides a new way of thinking to assess fatigue damage problems. The complete stress state at a certain material point, i.e., taking into account any material plane at that point, is included in the method. The influence of tension and compression state and also the mean stress are also included. Some experiments with different materials and loading conditions are used to validate the capabilities of the proposed method. The results show that the method provides good predictions for axial cyclic and/or torsion cyclic conditions with zero or nonzero mean stresses, in-phase and out-of-phase, different shapes of the specimen, loading waveform and loading path.
Autores:
Bergara, A.; Altuzarra, J.; Arredondo, A.; et al.
Revista:
ANALES DE LA MECANICA DE LA FRACTURA
ISSN:
0213-3725
Año:
2019
Vol.:
36
Págs.:
616 - 621
Revista:
INTERNATIONAL JOURNAL OF FATIGUE
ISSN:
0142-1123
Año:
2018
Vol.:
110
Págs.:
95 - 104
In this article, a universally applicable multiaxial fatigue criterion in 2D cyclic loading is proposed, which can be used for a great variety of materials and loading conditions. A strain-based fatigue parameter is defined and, at the same time, a new failure model is proposed to overcome the weaknesses of other mechanisms used previously. In addition, the influence of non-proportional loading, maximum, minimum and mean loading, the influence of both normal and shear components, Poisson effect, different failure types, etc. can also be taken into consideration. A huge number of materials and loading conditions are used to validate the capabilities of the proposed methodology. The results show that the new multiaxial fatigue criterion provides excellent life predictions for all the materials and loading conditions used in this work. The proposed approach can be regarded as a universally applicable multiaxial fatigue criterion in 2D cyclic loading.
Revista:
INTERNATIONAL JOURNAL OF FATIGUE
ISSN:
0142-1123
Año:
2018
Vol.:
113
Págs.:
78 - 87
A multiaxial fatigue criterion recently developed by the authors for 2D conditions is extended here to 3D situations and applied to predict fatigue damage in rail welded joints with the help of an explicit finite element model. Contact theory and axle box acceleration response in frequency domain are used to validate the finite element model. The influence of depth and length of the welded joints is analyzed. It is found that fatigue damage is more severe with shorter and deeper welded joints. When the length of the welded joints is less than 150 mm, fatigue damage is greatly increased with the increasing of the depth. When the depth is less than 0.1 mm, fatigue damage is not relevant, regardless of the length. When the depth is greater than 0.3 mm, fatigue damage increases significantly with the decreasing of the joint length, especially when the length is less than 150 mm. When the welded joints are long enough, the depth restriction can be relaxed. This work can provide guidance and theoretical support for maintenance and repair of rail welded joints.
Revista:
ANALES DE LA MECANICA DE LA FRACTURA
ISSN:
0213-3725
Año:
2018
Vol.:
35
Págs.:
52 - 57
La vida a fatiga de los componentes aeronáuticos rotativos que trabajan a elevadas temperaturas dentro de la turbina de
un motor de aviación es un factor crítico de diseño. Las condiciones en las que se mecanizan componentes como los
discos de turbina en estas aleaciones de base níquel, por ejemplo, discos de turbina, afectan a su posterior vida en servicio.
Los procesos de mecanizado de distintas zonas (torneado, brochado¿) afectan a la rugosidad superficial, daño y capa
superficial deformada (incluyendo los efectos de posibles carburos rotos) y a la distribución de las tensiones residuales
próximas a la superficie. Por añadidura, es posible aplicar o no un tratamiento posterior de granallado que modifica la
integridad superficial. El propósito de este trabajo es ser capaz de separar los efectos que tienen las diferentes variables:
rugosidad, espesor de la capa afectada por el mecanizado y las tensiones residuales; de modo que se puedan optimizar
tanto las condiciones del mecanizado como la vida en fatiga de los componentes.
Revista:
INTERNATIONAL JOURNAL OF FATIGUE
ISSN:
0142-1123
Año:
2018
Vol.:
108
Págs.:
109 - 115
A new multiaxial fatigue criterion is proposed that takes into account the influence of material properties and loading conditions on the direction of the critical fatigue plane. Poisson's effect, normal and shear strain energies, both elastic and plastic, and material hardening can be taken into account in this criterion. Ten different materials subjected to various loading paths with different test-sample geometries are used to validate the capabilities of the proposed approach. The comparison with other commonly used energy-based criteria is also presented. The results show that the proposed criterion provides very good predictions for all the analysed materials and loading conditions (within a factor of two) used in this work. The error in life prediction with the present approach also compares favourably with respect to other criteria available in the literature.
Revista:
INTERNATIONAL JOURNAL OF FATIGUE
ISSN:
0142-1123
Año:
2018
Vol.:
114
Págs.:
323 - 330
A multiaxial fatigue criterion is proposed, which can be seen as a modification of a previous criterion presented by the authors. The influence of the unique material state can be taken into consideration, as well as the range and mean value of the variables involved in the fatigue parameter for depicting the influence of the loading condition. Definitions of the out-of-phase failure and out-of-phase failure angle are proposed, as well as an out of-phase failure parameter that can be used to express the interdependent relationship with the out-of-phase failure, in both normal-type and shear-type failure. An explicit physical interpretation of different failure types is proposed. After validation and comparison with experimental results for different loading conditions and materials, it is concluded that the prediction ability of this modified multiaxial fatigue criterion is better than that of the original Lu's criterion, as well as than those of the other commonly used multiaxial fatigue criteria.
Revista:
INTERNATIONAL JOURNAL OF FATIGUE
ISSN:
0142-1123
Año:
2017
Vol.:
103
Págs.:
112 - 121
This work presents the numerical simulation and validation of a fatigue propagation test of a semi elliptical crack located at the side of the rectangular section of a beam subjected to four-point bending. For most common fatigue test configurations there are equations that allow calculating the stress intensity factors (SIFs). However, no solution is provided if the crack is located on any of the lateral sides of the rectangular section, since one part of the crack is located in the tractive zone while the other is at the compressive zone. In these cases, it is necessary to use alternative methods. The Extended Finite Element Method (XFEM) provides a new alternative for the calculation of SIFs, and to simulate crack propagation, by using special interpolation functions. Furthermore, XFEM-based LEFM approach offers the advantage of performing crack growth analysis without the need for updating the mesh (re meshing). The experimental tests have been carried out in an Instron 8874 biaxial testing machine. Crack growth was controlled by optical microscopy and by progressive crack surface heat tinting. For the numerical simulations, the Extended Finite Element Method (XFEM) implemented in the Abaqus (R) 2017 software has been used. The comparison between the experimental and numerical results shows very good correlation regarding crack shape and number of cycles to failure. The capabilities of the XFEM-based LEFM approach to simulate fatigue crack growth in complex crack fronts are validated. (C) 2017 Elsevier Ltd. All rights reserved.
Revista:
INTERNATIONAL JOURNAL OF FATIGUE
ISSN:
0142-1123
Año:
2017
Vol.:
104
Págs.:
99 - 111
A new approach for the definition of the critical plane and a new energy-based multiaxial fatigue parameter are proposed in this work. The normal strain energy and shear strain energy on two orthogonal material planes are used to predict fatigue damage in multiaxial fatigue loading. The influence of the Poisson effect, mean normal strain energy and the different contribution of the compressive and tensile normal strain energies are accounted for. An energy-based parameter is defined which explains the different effects of the total strain energy on different material directions. Experimental data are used to validate the capabilities of this new multiaxial fatigue parameter, including 10 materials and 33 loading paths, which cover most of the commonly used loading conditions in multiaxial fatigue tests. The results show that the proposed multiaxial fatigue parameter gives good predictions (within a life factor of two) for most of these materials and loading paths. (C) 2017 Elsevier Ltd. All rights reserved.
Revista:
FATIGUE AND FRACTURE OF ENGINEERING MATERIALS AND STRUCTURES
ISSN:
8756-758X
Año:
2017
Vol.:
40
N°:
12
Págs.:
1994 - 2007
A new method for predicting crack plane direction in high-cycle multiaxial fatigue is proposed. This method considers material properties and loading conditions. Two situations are considered: (i) in-phase loading, where the crack plane direction only depends on the loading condition and material properties have little influence on it, and (ii) out-of-phase loading, where the crack plane direction is affected by both loading conditions and material properties. The prediction accuracy is assessed by comparison with several experimental results, including different loading conditions and materials. The results show that the proposed method provides a good prediction capability for these experiments.
Revista:
FUSION ENGINEERING AND DESIGN
ISSN:
0920-3796
Año:
2017
Vol.:
124
Págs.:
958 - 963
Flow Channel Inserts (FCIs) are key elements in a DCLL blanket concept for DEMO, since they provide the required thermal insulation between the He cooled structural steel and the hot liquid PbLi flowing at approximate to 700 degrees C, and the necessary electrical insulation to minimize MHD effects. In this work a SiC-based sandwich material is proposed for FCIs, consisting of a porous SiC core covered by a dense CVD-SiC layer. A method to produce the porous SiC core is presented, based on combining a starting mixture of SiC powder with a spherical carbonaceous sacrificial phase, which is removed after sintering by oxidation, in such a way that a microstructure of spherical pores is achieved. Following this technique, a porous SiC material with low thermal and electrical conductivities, but enough mechanical strength was produced. Samples were covered by a 200 mu m thick CVD-SiC coating to form a SiC-sandwich material. Finally, corrosion tests under static PbLi were performed, showing that such a dense layer offers a reliable protection against static PbLi corrosion. (C) 2017 Elsevier B.V. All rights reserved.
Revista:
NUCLEAR MATERIALS AND ENERGY
ISSN:
2352-1791
Año:
2016
Vol.:
7
Págs.:
5 - 11
The Dual Coolant Led Lithium (DCLL) blanket is one of the concepts being investigated as candidate for DEMO, due to the high thermal efficiency provided by the flowing PbLi self-cooled breeder at approximate to 700 degrees C in the high temperature design. Key elements are the Flow Channel Inserts (FCIs) serving as electrical and thermal insulators to mitigate MHD effects and to keep the He-cooled steel walls below its maximum allowable temperature due to corrosion. A material based on sandwiching porous SiC between dense SiC layers is proposed for FCIs. In this work results of theoretical calculations and an FEM model are presented to determine the optimum thickness of both porous core and outer dense layers to assure the required thermal insulation across the FCI with minimum thermal stresses, considering achievable properties for the porous SiC material and its fabrication possibilities. It is concluded that the porous core thickness must be at least 5 mm if a porous SiC with thermal conductivity around 7 W/mK is used; a dense coating of approximate to 200 mu m is considered as optimum regarding the thermal stresses present in the FCI.
Revista:
INTERNATIONAL JOURNAL OF REFRACTORY METALS AND HARD MATERIALS
ISSN:
0263-4368
Año:
2014
Vol.:
43
Págs.:
236 - 240
Microbeam testing is proposed as a new method for analysing the mechanical properties of individual microstructural features in WC-Co hardmetals; i.e. portions of WC grains or a single metallic ligament. Firstly, cantilever microbeams with dimensions below the microstructural scale of the material are machined by means of a focused ion beam (FIB). Afterwards, these beams are bended to fracture by means of an instrumented nanoindenter. In this way, both portions of WC grains and binder phase ligaments are broken while simultaneously recording the load and the vertical displacement of the nanoindenter tip. These cracking events are detected as sudden steps in the load vs. displacement curves. Afterwards, a scanning electron microscope is used to measure the distance from the main crack to the beam clamping. From these data, the stresses at which portions of cobalt ligaments and WC grains fail are estimated from linear elastic theory and FEM models.
Revista:
THIN SOLID FILMS
ISSN:
0040-6090
Año:
2014
Vol.:
571
Págs.:
296 - 301
Microelectronic industry is driven by the continuous miniaturization process conducing to the introduction of materials with better performance. These materials are subjected to stresses mainly due to thermal mismatch, microstructural changes or process integration which can be in the origin of mechanical reliability issues. To study these phenomena and even electromigration a good mechanical characterization of the materials is needed. This work aims at developing tests to assess fracture and elastoplastic behavior of thin Cu films. The tests developed are based on the deflection of microbeams (micromachined using a focused ion beam) using a nanoindenter. Different test geometries for microbeams have been evaluated and quantitative data have been obtained combining experimental results with analytical or numerical models, depending on the property under study. Microbeam response shows a strong dependence on the orientation of the grains close to the fixed end. Grain orientation has been measured by electron backscatter diffraction and the plastic behavior has been modeled by the finite element method using an in-house crystal plasticity subroutine. The effect of film thickness on fracture energy has been determined from tests of notched beams. (C) 2014 Elsevier B.V. All rights reserved.
Revista:
THIN SOLID FILMS
ISSN:
0040-6090
Año:
2014
Vol.:
564
Págs.:
314 - 320
The continuous miniaturization process in the microelectronic industry, along with the introduction of Interlayer Dielectrics (ILDs) with poorer mechanical properties, makes necessary the development of characterization techniques to evaluate the mechanical performance of very thin films. This work presents a mechanical characterization technique for thin films based on membrane testing. Membranes, micromachined with anisotropic wet etching of Si, are tested to fracture using a nanoindenter to apply the load and register the provoked deflection. The technique is applied to the fracture characterization of two different ILDs with four thicknesses ranging from 100 nm to 500 nm. Combination of experiments and finite element simulations allows for the calculation of the strength of the materials from the fracture load. The technique permits to discriminate both ILDs and to establish clear thickness dependence: for both materials, 100 nm films show a significant lower strength while no effect of film thickness on strength is observed in the range between 200 and 500 nm. A sensitivity analysis of the outcome of the technique, the fracture stress, to the variability of the input parameters is presented, showing the robustness of the proposed approach: the experimental error in the fracture stress is smaller than the variation in the input parameters.
Revista:
ACTA MATERIALIA
ISSN:
1359-6454
Año:
2014
Vol.:
71
Págs.:
44 - 55
The continuous process of miniaturization in the microelectronics industry requires the introduction of new, thinner interlayer dielectric (ILD) materials with poorer mechanical properties. As a consequence, new mechanical characterization techniques are needed in the industry to evaluate very thin films. This work presents a new fracture characterization technique for thin films, called "dual tip indentation" (DTI). The technique takes advantage of a particular geometry of the indentation tip to provoke shallow and controlled cracking on the targeted brittle thin film. The technique is applied to the fracture characterization of two different ILD with four thicknesses, ranging from 100 nm to 500 nm. Further fractographic analysis, along with finite element modeling, shows that it is possible to extract intrinsic fracture properties from the fracture load. The technique allows one to discriminate between the ILD and, for both materials, 100 nm films show lower strength. No effect of film thickness on strength is observed in the range between 200 and 500 nm. The results from DTI compare well with those previously obtained for the same materials from membrane testing, taking into account the differences in volume tested.
Revista:
COMPUTATIONAL MATERIALS SCIENCE
ISSN:
0927-0256
Año:
2014
Vol.:
82
Págs.:
314 - 319
This work presents a finite element analysis of the indentation size effect (ISE) experimentally observed in tests performed at submicron scale. A 3D model of a conical rigid surface indenting on a Nb single crystal at different depths has been developed. The bcc Nb material has been characterized within a finite-strain framework through a crystal plasticity model incorporating strain-gradient hardening. The hardness evolution for different material orientations and for different initial dislocation densities has been studied. The numerical results are compared with predictions of existing analytical models and with experimental results. (C) 2013 Elsevier B.V. All rights reserved.
Revista:
MATHEMATICS AND COMPUTERS IN SIMULATION
ISSN:
0378-4754
Año:
2011
Vol.:
81
N°:
11
Págs.:
2564 - 2580
Liquid-phase sintering (LPS) is a consolidation process for metallic and ceramic powders. At given temperature conditions, the process occurs with constant amount of liquid phase. However, the evolution of solid-particle shape is observed, namely, the rounding of particles and the growth of big particles at the expense of the small ones, which is known as Ostwald ripening. In this work, we propose a Monte Carlo (MC) model to simulate the microstructural evolution during LPS. The model considers the change of state of the discretising elements, namely voxels, of the system. The microstructural evolution proceeds accounting for both the geometrical characteristics of the particles, such as the number of solid neighbours, and the amount of solute contained in or surrounding a randomly chosen voxel. This has been implemented in terms of two probability distribution functions (PDFs). The diffusion of solute has also been considered by means of the implementation of a three-dimensional finite-difference algorithm. The diffusional MC model that we present is able to reproduce the Ostwald ripening behaviour and, in particular, results match the case in which the process is limited by the diffusion of the solute in the liquid phase. (C) 2011 IMACS. Published by Elsevier B.V. All rights reserved.
Revista:
PHILOSOPHICAL MAGAZINE
ISSN:
1478-6435
Año:
2011
Vol.:
91
N°:
42620
Págs.:
1400 - 1408
Unloading stiffness is a critical magnitude when extracting elastic modulus in instrumented indentation. Any phenomenon which interacts with its measurement may affect the final calculation of the modulus. Analytical and numerical calculations have been carried out to determine the influence of thermal drift and creep response on its measurement, and the predictions were in good agreement with experimental results. Since the influence of thermal drift is depth-dependent, it determines the effective resolution of an indentation device for a given material. In contrast, indentation creep significantly alters unloading stiffness even for weakly rate-sensitive materials (sensitivity exponent, m < 0.05) but its effect could be smoothed down due to measurement artefacts (unloading curve fitting strategy). For instance, for an ultra-fine grained (UFG) pure niobium at room temperature (m similar to 0.015 and H/E(r) similar to 0.02), the error in the measurement of elastic modulus with a typical nanoindentation procedure (5 s of holding time and 65 s of unloading time) can be as high as 15%. This paper proposes simple rules for a reliable experimental procedure to avoid both thermal drift and creep effects on the measurement of elastic modulus, which are especially relevant for the new generation of high temperature instrumented indentation facilities.
Revista:
MATHEMATICS AND COMPUTERS IN SIMULATION
ISSN:
0378-4754
Año:
2010
Vol.:
80
N°:
7
Págs.:
1469 - 1486
Liquid-phase sintering (LPS) is an industrial process used to consolidate materials composed of two different kinds of metallic and/or ceramic powders. At constant temperature, the amount of the present liquid-phase is constant However, the shape of particles of solid phase changes over time In general, the rounding of particles and the growth of big particles at the expense of the small ones are observed This process is known as Ostwald ripening. In this work, we propose a Monte Carlo (MC) model to simulate the microstructural evolution during LPS The discretizing elements of the system. namely the voxels. change state between solid and liquid. according to previously defined melting and solidification probability distribution functions (PDFs) The generated PDFs take into account the geometrical characteristics of the system particles in terms of number of solid neighbours that surround a randomly chosen voxel The geometrical MC model that we present is able to reproduce the Ostwald ripening behaviour and, in particular, matches the case in which the process occurs limited by the attachment/detachment of the solid phase to/from the surface of the particle (C) 2009 IMACS Published by Elsevier B V All rights reserved.
Revista:
PHILOSOPHICAL MAGAZINE
ISSN:
1478-6435
Año:
2010
Vol.:
90
N°:
27-28
Págs.:
3743 - 3756
We present molecular dynamics (MD) simulations of the shear-coupled migration (SCM) behaviour of symmetrical tilt boundaries perturbed by the presence of nano-cracks or nano-precipitates lying on the boundary plane. The simulations have been performed for copper bicrystals at room temperature (300 K). The tilt boundary gets pinned by the crack tip or precipitates; shear-coupled migration occurs only ahead of the pinning points. Bulging of the tilt boundary reduces the shear stress on the boundary surface near the pinning points. In the case of cracks, the local deviation of the boundary from the crack plane close to the crack tip hinders mode II crack propagation; in fact, crack healing is observed in some cases. The applied stress grows until depinning of the boundary takes place by SCM bulging or by the combined action of SCM with another deformation mechanism (emission of dislocations from the pinning point vicinity, grain boundary sliding).
Revista:
ENGINEERING FAILURE ANALYSIS
ISSN:
1350-6307
Año:
2010
Vol.:
17
N°:
1
Págs.:
48 - 60
What is the optimum cross-section for a compression member built by bending a plate of a given thickness and area? It is shown that a parabolic shape is 41% better than a tubular section. A number of examples are shown where this section is found in nature. (C) 2008 Elsevier Ltd. All rights reserved.
Revista:
ENGINEERING FAILURE ANALYSIS
ISSN:
1350-6307
Año:
2010
Vol.:
17
N°:
1
Págs.:
226 - 235
The fatigue behaviour of next generation high strength steels (sigma(UTS) = 950-1000 MPa) has been studied. Specifically, this study is focused on the initiation stage of fatigue micro-cracks. With this purpose, high cycle fatigue tests under uniaxial loading have been performed. During these tests, the deformation history of the specimen has been tracked by means of speckle interferometry. This technique allows monitoring the evolution of the displacement field and its derivatives on the specimen surface, so that it can be used as a tool for detecting microcracks in the first stages of crack initiation. The observation of the fracture surfaces provides complementary information about the localization of the initiation of failure thus, a correlation between the observations made by interferometry and the actual location of the fatigue nucleus and the evolution of the crack during its propagation can be established. Results appoint speckle interferometry as a promising technique for the detection of fatigue failures. (C) 2009 Elsevier Ltd. All rights reserved.